NMR Crystallography
496NMR Crystallography
496eBook
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Overview
The handbook is organized into six parts. The first contains an overview and some chapters on fundamental NMR topics. Next comes a part concentrating on chemical shifts, followed by one on coupling interactions. Part D contains chapters describing how NMR results relate to fundamental crystallography concepts and to diffraction methods. The fifth part concerns specific of structure, such as hydrogen bonding, and also has chapters on questions of molecular-level mobility ad phase transitions. Finally, the four chapters in the last part give applications of NMR crystallography to structural biology, organic and pharmaceutical chemistry, inorganic and materials chemistry, and geochemistry.
Product Details
ISBN-13: | 9781118587324 |
---|---|
Publisher: | Wiley |
Publication date: | 12/19/2012 |
Series: | eMagRes Books |
Sold by: | JOHN WILEY & SONS |
Format: | eBook |
Pages: | 496 |
File size: | 20 MB |
Note: | This product may take a few minutes to download. |
About the Author
Roderick Wasylishen, Professor, University of Alberta, Edmonton, Alberta, CANADA.
Dr Melinda Duer, Department of Chemistry, University of Cambridge, UK.
Table of Contents
Contributors.Series Preface.
Volume Preface.
Part A: Introduction.
1 Crystallography & NMR: an Overview (Robin K. Harris).
2 Tensors in NMR (S. Chandra Shekar, Alexej Jerschow).
3 Computation of Magnetic Resonance Parameters for Crystalline Systems: Principles (Jonathan R. Yates, Chris J. Pickard).
4 Experimental Characterization of Nuclear Spin Interaction Tensors (Jeremy J. Titman).
Part B: Chemical Shifts.
5 Magnetic Shielding & Chemical Shifts: Basics (Julio C. Facelli, Anita M. Orendt).
6 Symmetry Effects at the Local Level (Matthias Bechmann, Angelika Sebald).
7 Chemical Shift Computations for Crystalline Molecular Systems: Practice (Robin K. Harris, Paul Hodgkinson, Chris J. Pickard, Jonathan R. Yates, Vadim Zorin).
8 Chemical Shifts & Solid-state Molecular-level Structure (Anita M. Orendt, Julio C. Facelli).
9 Chemical Shift Anisotropy & Asymmetry: Relationships to Crystal Structure (James K. Harper).
Part C: Coupling Interactions.
10 Dipolar & Indirect Coupling: Basics (Roderick E. Wasylishen).
11 Dipolar Recoupling: Heteronuclear (Christopher P. Jaroniec).
12 Dipolar Recoupling: Homonuclear (Robert Tycko).
13 Dipolar Coupling: Molecular-level Mobility (Detlef Reichert, Kay Saalwächter).
14 Spin Diffusion in Crystalline Solids (Lyndon Emsley).
15 Indirect Coupling & Connectivity (Anne Lesage).
16 Nuclear Quadrupole Coupling: An Introduction & Crystallographic Aspects (Sharon E. Ashbrook, Stephen Wimperis).
Part D: Crystal Structure Determination using NMR.
17 Fundamental Principles of NMR Crystallography (Francis Taulelle).
18 Interplay between NMR & Single-crystal X-ray Diffraction (Darren H. Brouwer).
19 Combined Analysis of NMR & Powder Diffraction Data (Kenneth D.M. Harris, Mingcan Xu).
20 Tensor Interplay (David L. Bryce).
Part E: Properties of the Crystalline State.
21 Intermolecular Interactions & Structural Motifs (Lindsay S. Cahill, Gillian R. Goward).
22 Hydrogen Bonding in Crystalline Organic Solids (Steven P. Brown).
23 Inorganic Non-stoichiometric Crystalline Systems & Atomic Ordering (Mark E. Smith).
24 Rotational & Translational Dynamics (Christopher I. Ratcliffe).
25 Intramolecular Motion in Crystalline Organic Solids (Paul Hodgkinson).
26 Structural Phase Transitions (Kenneth R. Jeffrey, Glenn H. Penner).
Part F: Applications of NMR to Crystalline Solids.
27 Structural Biology (David A. Middleton).
28 Organic & Pharmaceutical Chemistry (Marek J. Potrzebowski).
29 Inorganic & Materials Chemistry (Ray Dupree).
30 Geochemistry (Brian L. Phillips).
Index.
What People are Saying About This
“In summing up my book review, I would again quote Professor Harris from reference (2): ‘Perhaps now is the time to consider constituting a division of NMR crystallography within the International Union of Crystallography. Certainly a formal or semi-formal link with the solid-state NMR community is desirable’. Forearmed with this book, I would support that proposal. This book, I would also conclude, should be in the library of crystallographic laboratories, across all the disciplines.” (Crystallography Reviews, 14 February 2012)